TG-FTIR Thermogravimetric Analysis

TG-FTIR Thermogravimetric Analysis

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Thermal Analysis provides ideal tools for the characterization of organic and inorganic, either solids or liquids. Thermodynamic transitions, thermal stability, decomposition and chemical reactions can be detected and quantified with high accuracy over a broad temperature range

The identification of gases released directly from the sample or during thermal treatment cannot be performed just by thermal analysis, but coupling a spectroscopic method such as Fourier-Transform-Infrared (FT-IR) spectroscopy is an excellent solution.

Categories: FT-IR Research Spectrometers, FTIR, Infrared & Near Infrared

Description

 

Category Details
Technique Overview IR spectroscopy depends on interaction of infrared radiation with vibrating dipole moments of molecules, Gives characteristic spectrum for each substance (except homonuclear diatomics and noble gases), Combines quantitative capabilities of TG with identification capabilities of FT-IR spectroscopy
Three Coupling Modes External coupling via transfer line, Internal coupling via transfer line, Direct PERSEUS® coupling without transfer line
External Coupling Equipped with additional detector (DLaTGS room temperature or liquid nitrogen cooled MCT), Simple computer controlled switch for either sample compartment measurements or combined TG-FT-IR analysis, Highest FT-IR system flexibility
Internal Coupling Detection sensitivity follows Beer’s law, Sensitivity depends on path length of cell, concentration, and absorptivity of molecule, Longer path length allows more molecules to pass through, Lower cell volume results in higher concentration of evolved gases, Balance between path length, cell volume, and sample amount
PERSEUS® Coupling Patented alliance between ALPHA II FT-IR spectrometer and NETZSCH Thermoanalyzers, Direct coupling without transfer line, Tiny and efficient design

 

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