Bruker FM: MIR-FIR/THz in one go

Bruker FM: MIR-FIR/THz in one go

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The extension of the mid IR towards the far IR spectral range below 400 cm-1 is of general interest for molecular vibrational analysis for various application fields and industry branches. Till now, to extend the spectral range, one or more additional far IR beamsplitters and detectors are required and the user has to manually open the spectrometer optics bench.

The unique Bruker FM technology for VERTEX 70v and INVENIO FT-IR research spectrometers which combines the wide spectral range beamsplitter, the wide range DTGS detector and the standard IR source to cover the spectral range from 6000 cm-1 down to 50 cm-1 (for INVENIO from 6000 cm-1 down to 80 cm-1) in one single scan for all types of transmittance, reflectance and ATR measurements.

 

 Additional Values of Bruker FM

  • Full mid and far IR spectrum in one go
  • Enormous time saving due to just one single measurement
  • Acquisition of the complete molecular vibrational spectral information
  • No break of purge or vacuum conditions for optical component exchange
  • No danger of touching or damaging expensive and sensitive optical components
  • No need for complex and demanding exchange devices
  • All optical components are insensitive to humidity
Categories: FTIR, Infrared & Near Infrared

Description

 

Category Details
Analysis of Polymer Fillers and Colored Pigments Only one measurement per sample for complete MIR-FIR/THz spectral range, Additional information on inorganic filler materials in polymers, Simple polymer identification using dedicated FIR-MIR library
Spectral Range Applications MID IR region (4000-400 cm-1) provides information about composition and structure of organic compounds, FIR/THz region (below 400 cm-1) provides information about lattice vibrations and vibrations of functional groups with heavy atoms in inorganic ionic compounds
Bruker FM Technology VERTEX 70v coverage: 6000-50 cm-1 in single scan, INVENIO coverage: 6000-80 cm-1 in single scan, Complete characterization of modern polymeric materials, Ideal tool for polymer composite analysis
Filler Material Identification Examples Polystyrene filled with titanium oxide, Acrylonitrile butadiene styrene copolymer filled with antimony trioxide
Polymorph Differentiation Identifies sample crystallinity, Same chemical compound can exist in different solid forms (crystals, solvates, desolvated solvates, amorphous solids), Different polymorphic forms have different physical properties (solubility, melting point, particle size, dissolution rate, hygroscopicity)
Polymorph Analysis Benefits MIR region covers fundamental molecular vibrations for substance identification, FIR region covers backbone vibrations of larger molecules and intermolecular vibrations in crystal lattices, Complete informative MIR-FIR/THz spectral range in one measurement, Important for pharmaceutical companies for bioavailability assessment
Polymorph Example Different antibiotic sulfathiazole polymorphs
Inorganic Minerals Applications Geology and metal organic chemistry, FIR/THz region important for inorganic substances with vibrations of heavier atoms, Characteristic bands below 400 cm-1, High quality far IR spectra obtained simultaneously with standard MIR spectra without changing optical components
ATR Accessory Simplifies sample preparation compared to traditional polyethylene discs and Nujol mulls in transmission mode, Platinum ATR accessory with diamond ATR crystal ideal for far IR operation, All reflective optics, OPUS software contains advanced ATR correction function for comparing FIR ATR results with reference transmission spectra
Inorganic Minerals Example CaCO3 FIR ATR measurement
MIR-FIR ATR Library First mid and far IR/Terahertz spectral library, Full FIR-MIR spectra (4000-30 cm-1), Compound information included, Ideal for studying filled polymer composites, Uses single crystal ATR technique, First library to extend lower limit from 400 cm-1 down to 30 cm-1, Enables creation of individual MIR-FIR ATR libraries for dedicated product or compound classes
Library Search Example Styrene Butadiene copolymer containing calcium carbonate

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